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Beilstein J. Org. Chem. 2016, 12, 1096–1100, doi:10.3762/bjoc.12.104
Graphical Abstract
Figure 1: Keramaphidin B (1).
Figure 2: Retrosynthetic analysis of keramaphidin B.
Scheme 1: Enantio- and diastereoselective bifunctional thiourea 12 organocatalysed Michael addition. (a) CO(O...
Scheme 2: Synthesis of bis alkene 5. (a) 12 (20 mol %), toluene, −20 °C, 36 h, 95:5 dr, 92% yield; (b) aq HCH...